三丁基(2-甲基苯基)锡烷合成路线 (共 36 条)
反应条件
cesium fluoride in ethanol; water
T=50°C; Stille coupling; 6 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Green Chemistry, 2010 , vol. 12, # 11 p. 2024 - 2029
反应条件
in dichloromethane
48 h; Heating;
参考文献
Cooper, Mark S.; Heaney Harry
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5011 - 5014
反应条件
in acetonitrile
25 h; Heating;
参考文献
Cooper, Mark S.; Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1989 , vol. 45, # 4 p. 1155 - 1166
反应条件
manganese(IV) oxide; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2; isopropyl alcohol
T=60°C; P=1292.9 Torr; 18 h;
参考文献
Gligorich, Keith M.; Iwai, Yasumasa; Cummings, Sarah A.; Sigman, Matthew S.
Tetrahedron, 2009 , vol. 65, # 26 p. 5074 - 5083
反应条件
Pd/Fe3O4; cesium fluoride in 1,4-dioxane
T=100°C; Stille Cross Coupling; 18 h;
参考文献
Prasad, Aviraboina Siva; Satyanarayana, Bollikonda
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 8 p. 2789 - 2792
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); cesium fluoride in tetrahydrofuran
T=50°C; Stille Cross Coupling; 8 h;
参考文献
Lee, Dong-Hwan; Qian, Yingjie; Park, Ji-Hoon; Lee, Jong-Suk; Shim, Sang-Eun; Jin, Myung-Jong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1729 - 1735