三丁基(3-甲基苯基)锡烷合成路线 （共 17 条）
反应条件
indium in neat (no solvent) T=20°C; 6 h; Inert atmosphereSonication; TemperatureTime; regioselective reaction;
参考文献
Lo Fiego, Marcos J.; Badajoz, Mercedes A.; Domini, Claudia; Chopa, Alicia B.; Lockhart, Maria T.
Ultrasonics Sonochemistry, 2013 , vol. 20, # 3 p. 826 - 832
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; Stille coupling; 0.5 h; Sonication;
参考文献
Domini, Claudia E.; Silbestri, Gustavo F.; Fernandez Band, Beatriz; Chopa, Alicia B.
Ultrasonics Sonochemistry, 2012 , vol. 19, # 3 p. 410 - 414
反应条件
sulfuryl dichloride T=20°C; 4 h;
参考文献
Chemische Berichte, , vol. 128, # 12 p. 1195 - 1198
反应条件
1: CH2Cl2 / 15 h / 20 °C 2: ice / CH2Cl2 / 0.5 h View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Chemische Berichte, 1991 , vol. 124, # 9 p. 1997 - 2000
反应条件
bis(η3-allyl-μ-chloropalladium(II)) T=20 - 65°C; Stille coupling; 16.25 h; Inert atmosphere;
参考文献
Lakshmi, B. Vasantha; Wefelscheid, Ulrike K.; Kazmaier, Uli
Synlett, 2011 , # 3 art. no. G36110ST, p. 345 - 348
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphere;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
bis(η3-allyl-μ-chloropalladium(II)) T=20 - 65°C; Stille coupling; 16.25 h; Inert atmosphere;
参考文献
Lakshmi, B. Vasantha; Wefelscheid, Ulrike K.; Kazmaier, Uli
Synlett, 2011 , # 3 art. no. G36110ST, p. 345 - 348
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 129, # 1 p. 45 - 51
反应条件
magnesium; ethylene dibromide in tetrahydrofuran
T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere; regioselective reaction;
参考文献
Gerbino, Dario C.; Fidelibus, Pablo M.; Mandolesi, Sandra D.; Ocampo, Romina A.; Scoccia, Jimena; Podesta, Julio C.
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 24 - 32
