2,5-二甲基-3-硝基苯甲醛合成路线 （共 4 条）
反应条件
hydrogenchloride; acetic acid in water
参考文献
Agence Nationale de Val orisation de la Recherche (ANVAR)
Patent: US4266060 A1, 1981 ;
反应条件
hydrogenchloride; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; acetic acid in water
2.5 h; Heating;
参考文献
Rivalle, Christian; Ducrocq, Claire; Lhoste, Jean-Marc; Bisagni, Emile
Journal of Organic Chemistry, 1980 , vol. 45, p. 2176 - 2180
反应条件
1: sulfuric acid; nitric acid / 0.33 h / 0 °C
2: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C
View Scheme
参考文献
VITAS PHARMA RESEARCH PVT LTD; ALAPATI, Chandrasekhar; BANERJEE, Ankita; RANGARAJAN, Radha; KUMAR, Rajinder
Patent: WO2014/57415 A2, 2014 ;
反应条件
piperidine in pyridine
24 h; Heating;
参考文献
Rivalle, Christian; Ducrocq, Claire; Lhoste, Jean-Marc; Bisagni, Emile
Journal of Organic Chemistry, 1980 , vol. 45, p. 2176 - 2180
