(7-碘[1,2,4]三氮唑并[1,5-A]吡啶)合成路线 （共 3 条）
反应条件
1: in DMF (N,N-dimethyl-formamide) T=130°C; 2: With hydroxylamine-o-sulphonic acid in pyridine; methanol T=0 - 20°C;
参考文献
WO2004/43940 A1, ;
Page 85 ;
反应条件
1: DMF / 12 h / 130 °C 2: 363 mg / pyridine; hydroxylamine-O-sulfonic acid / methanol / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 12 p. 3614 - 3627
反应条件
1: 97 percent / trifluoroacetic acid / CH2Cl2 / 1 h / 20 °C 2: DMF / 12 h / 130 °C 3: 363 mg / pyridine; hydroxylamine-O-sulfonic acid / methanol / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 12 p. 3614 - 3627
