反应条件
1: 61 percent / 80percent formic acid / 2 h / 100 - 110 °C
2: 93 percent / sodium borohydride / ethanol / 4 h / Ambient temperature
3: tert-butyl hydroperoxide, vanadium oxyacetylacetonate / benzene / 0.75 h / Ambient temperature
4: lithium aluminium hydride / tetrahydrofuran / 4 h
5: 92 percent / triethylamine, sulfur trioxide, pyridine / dimethylsulfoxide / 1 h / Ambient temperature
6: 65 percent / anhyd. AlCl3 / 0.05 h / 180 - 185 °C
View Scheme
参考文献
Tanno; Terashima
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 811 - 820