反应条件
1: pyridine / 2 h / Ambient temperature
2: POCl3, Et3N / CH2Cl2 / 8 h / -30 deg C to room temperature
3: tri-n-butylstannane, AIBN / toluene / 4 h / 85 °C
View Scheme
参考文献
Barton, Derek H. R.; Bringmann, Gerhard; Lamotte, Genevieve; Motherwell, William B.; Motherwell, Robyn S. Hay; Porter, Alexander E. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2657 - 2664