4-(2-氨基苯氧基)四氢-1(2H)-吡啶甲酸叔丁酯合成路线 （共 6 条）
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=3750.38 Torr; 2 h;
参考文献
PIERRE FABRE MEDICAMENT; Dupont-Passelaigue, Elisabeth; Le Roy, Isabelle; Pignier, Christophe
Patent: US2013/172326 A1, 2013 ;
Location in patent: Paragraph 0136 ;
反应条件
1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C 2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr View Scheme
反应条件
1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C 2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr View Scheme
反应条件
hydrogen; palladium on activated charcoal in methanol
T=20°C; P=3750.38 Torr; 2 h;
参考文献
PIERRE FABRE MEDICAMENT; DUPONT-PASSELAIGUE, Elisabeth; LE ROY, Isabelle; PIGNIER, Christophe
Patent: WO2012/69503 A1, 2012 ;
Location in patent: Page/Page column 25 ;
反应条件
1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C
2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr
View Scheme
参考文献
PIERRE FABRE MEDICAMENT; DUPONT-PASSELAIGUE, Elisabeth; LE ROY, Isabelle; PIGNIER, Christophe
Patent: WO2012/69503 A1, 2012 ;
反应条件
1: triphenylphosphine; diethylazodicarboxylate / 2 h / 20 °C
2: hydrogen / palladium on activated charcoal / methanol / 2 h / 20 °C / 3750.38 Torr
View Scheme
参考文献
PIERRE FABRE MEDICAMENT; DUPONT-PASSELAIGUE, Elisabeth; LE ROY, Isabelle; PIGNIER, Christophe
Patent: WO2012/69503 A1, 2012 ;
