4-(羟甲基)苯甲酸甲酯合成路线 （共 132 条）
参考文献
Tai, Chih-Ho; Wu, Hsiao-Ching; Li, Wen-Ren
Organic Letters, 2004 , vol. 6, # 17 p. 2905 - 2908
反应条件
[Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; hydrogen in ethanol T=80°C; 36 h;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 39 p. 9851 - 9855
反应条件
1: 84 percent / NaBH4 / methanol / 2 h / 20 °C 2: 83 percent / thionyl chloride / 3 h / 50 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 12 p. 1964 - 1972
反应条件
1: pyrrolidine With formic acid 0.25 h; cooling; 2: 4-formylbenzoic acid methyl ester T=180 - 200°C; Leuckart-Wallach reaction; 8 h; Further stages.;
参考文献
Ignatovich; Gusak; Chernikhova; Kozlov; Koroleva
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 12 p. 1540 - 1543
反应条件
1: morpholine With formic acid 0.25 h; cooling; 2: 4-formylbenzoic acid methyl ester T=180 - 200°C; Leuckart-Wallach reaction; 8 h; Further stages.;
参考文献
Ignatovich; Gusak; Chernikhova; Kozlov; Koroleva
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 12 p. 1540 - 1543
反应条件
Amberlyst A-26 bicarbonate form; Amberlyst A-26 iodide form in various solvent(s) 3 h; Heating;
参考文献
Ruddick, Clare L.; Hodge, Philip; Houghton, Mark P.
Synthesis, 1996 , # 11 p. 1359 - 1362
反应条件
1: sodium tetrahydroborate / methanol / 0.17 h / 20 °C / Inert atmosphere 2: copper(II) bis(trifluoromethanesulfonate) / 16 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 27 p. 6175 - 6177
反应条件
sodium tetrahydroborate in ethanol UV-irradiation; chemoselective reaction;
参考文献
Journal of the Iranian Chemical Society, , vol. 11, # 1 p. 147 - 154
反应条件
(electrochemical reduction);
参考文献
Justus Liebigs Annalen der Chemie, , p. 2036 - 2066
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 32 p. 5687 - 5690
