(R)-(+)-1,2-环氧基十六烷合成路线 （共 7 条）
反应条件
sodium methylate in methanol
1 h; Ambient temperature;
参考文献
Jacoby, Claude; Braekman, Jean-Claude; Daloze, Desire
Tetrahedron, 1996 , vol. 52, # 31 p. 10473 - 10484
反应条件
(R,R)-(-)-(Salen)Co(III); water in tetrahydrofuran
T=0°C; 6 h;
参考文献
Lafont, Dominique; Bouchu, Marie-Noelle; Girard-Egrot, Agnes; Boullanger, Paul
Carbohydrate Research, 2001 , vol. 336, # 3 p. 181 - 194
反应条件
1: 70percent aq. CF3CO2 / CH2Cl2 / 1 h / 0 °C
2: 65 percent / NaBH4 / methanol / 0.5 h / Ambient temperature
3: 84 percent / MeONa / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Jacoby, Claude; Braekman, Jean-Claude; Daloze, Desire
Tetrahedron, 1996 , vol. 52, # 31 p. 10473 - 10484
反应条件
1: 65 percent / NaBH4 / methanol / 0.5 h / Ambient temperature
2: 84 percent / MeONa / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Jacoby, Claude; Braekman, Jean-Claude; Daloze, Desire
Tetrahedron, 1996 , vol. 52, # 31 p. 10473 - 10484
反应条件
Jacobsen catalyst in tetrahydrofuran; water
36 h; Title compound not separated from byproducts.;
参考文献
Chandrasekhar; Rambabu; Reddy, A. Syamprasad
Tetrahedron Letters, 2008 , vol. 49, # 29-30 p. 4476 - 4478
参考文献
Savle, Prashant S.; Lamoreaux, Marika J.; Berry, John F.; Gandour, Richard D.
Tetrahedron Asymmetry, 1998 , vol. 9, # 11 p. 1843 - 1846
参考文献
Lafont, Dominique; Bouchu, Marie-Noelle; Girard-Egrot, Agnes; Boullanger, Paul
Carbohydrate Research, 2001 , vol. 336, # 3 p. 181 - 194
