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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
69111-76-8
合成路线
（共 7 条）
67282-55-7
1-甲氧基-1H-吲哚-3-甲醛
+
75-52-5
硝基甲烷
→
反应条件
69111-76-8
反应条件
ammonium acetate Henry Nitro Aldol Condensation; 2 h; Reflux;
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
54698-11-2
1-甲氧基-1H-吲哚
+
73430-27-0
→
反应条件
69111-76-8
反应条件
in acetonitrile; trifluoroacetic acid
参考文献
Somei, Masanori; Sato, Haruhiko; Komura, Naoko; Kaneko, Chikara
Heterocycles, 1985 , vol. 23, # 5 p. 1101 - 1106
88-72-2
2-硝基甲苯
→
反应条件
69111-76-8
反应条件
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 35 h / |Reflux 2.1: water; zinc; ammonium chloride / diethyl ether / 4 h / 20 °C 3.1: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C 4.1: trichlorophosphate / |Cooling with ice 4.2: 3 h / 20 °C 4.3: |Cooling with ice 5.1: ammonium acetate / 2 h / |Reflux View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
20973-67-5
→
反应条件
69111-76-8
反应条件
1.1: water; zinc; ammonium chloride / diethyl ether / 4 h / 20 °C 2.1: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C 3.1: trichlorophosphate / |Cooling with ice 3.2: 3 h / 20 °C 3.3: |Cooling with ice 4.1: ammonium acetate / 2 h / |Reflux View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
3289-82-5
→
反应条件
69111-76-8
反应条件
1.1: Aliquatreg; 336; sodium hydroxide / diethyl ether; water / 21 h / 20 °C 2.1: trichlorophosphate / |Cooling with ice 2.2: 3 h / 20 °C 2.3: |Cooling with ice 3.1: ammonium acetate / 2 h / |Reflux View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
54698-11-2
1-甲氧基-1H-吲哚
→
反应条件
69111-76-8
反应条件
1.1: trichlorophosphate / |Cooling with ice 1.2: 3 h / 20 °C 1.3: |Cooling with ice 2.1: ammonium acetate / 2 h / |Reflux View Scheme
参考文献
Vo, Quan V.; Trenerry, Craige; Rochfort, Simone; Wadeson, Jenny; Leyton, Carolina; Hughes, Andrew B.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 856 - 864
69111-76-8
→
反应条件
20127-61-1
反应条件
1: 62 percent / lithium aluminum hydride / diethyl ether / Heating 2: 81 percent / Et3N / CH2Cl2 3: 63 percent / phosphoryl chloride / 0.33 h / 110 °C 4: 10 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH2Cl2 / Ambient temperature View Scheme
参考文献
Somei, Masanori; Sato, Haruhiko; Komura, Naoko; Kaneko, Chikara
Heterocycles, 1985 , vol. 23, # 5 p. 1101 - 1106
