反-11-二十碳烯酸甲酯合成路线 （共 12 条）
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
反应条件
methanesulfonyl chloride in ethanol; water
T=22°C; γ-Irradiation; G-values;
参考文献
Tamba, Maurizio; Dajka, Katalin; Ferreri, Carla; Asmus, Klaus-Dieter; Chatgilialoglu, Chryssostomos
Journal of the American Chemical Society, 2007 , vol. 129, # 28 p. 8716 - 8723
反应条件
1: CCl4; PBr3 / anfangs unter Kuehlung, zuletzt unter Erwaermen
2: absolute ethanol / Verseifen der Reaktionsprodukte mit 50prozentiger KOH und Destillieren der erhaltenen Dicabonsaeure unter vermindertem Druck
3: H2SO4
View Scheme
参考文献
Fieser; Chamberlin
Journal of the American Chemical Society, 1948 , vol. 70, p. 74
反应条件
1: absolute ethanol / Verseifen der Reaktionsprodukte mit 50prozentiger KOH und Destillieren der erhaltenen Dicabonsaeure unter vermindertem Druck
2: H2SO4
View Scheme
参考文献
Fieser; Chamberlin
Journal of the American Chemical Society, 1948 , vol. 70, p. 74
反应条件
1: sodium; butyl alcohol
2: CCl4; PBr3 / anfangs unter Kuehlung, zuletzt unter Erwaermen
3: absolute ethanol / Verseifen der Reaktionsprodukte mit 50prozentiger KOH und Destillieren der erhaltenen Dicabonsaeure unter vermindertem Druck
4: H2SO4
View Scheme
参考文献
Fieser; Chamberlin
Journal of the American Chemical Society, 1948 , vol. 70, p. 74
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
反应条件
sulfuric acid in water
T=80°C; 4 h;
参考文献
Napolitano, Assunta; Carbone, Virginia; Saggese, Paola; Takagaki, Kinya; Pizza, Cosimo
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 25 p. 10289 - 10297
