N-正丁基-1,8-萘二甲酰亚胺合成路线 （共 10 条）
参考文献
Wu, Qiang; Qin, Wen
Asian Journal of Chemistry, 2011 , vol. 23, # 10 p. 4713 - 4714
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=70°C; 0.166667 h; Microwave irradiation;
参考文献
Escudero, Mercedes Isasmendi; Kremenchuzky, Lautaro D.; Perillo, Isabel A.; Cerecetto, Hugo; Blanco, Maria M.
Synthesis, 2011 , # 4 art. no. M06310SS, p. 571 - 576
反应条件
amine Vs or Vt
T=200°C; 0.333333 h;
参考文献
Ganin, E. V.; Makarov, V. F.; Nikitin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2209 - 2215
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2415 - 2423
反应条件
sodium hydroxide in water
T=30°C; 24 h;
参考文献
De Barros, Teresa Cristina; Filho, Pedro Berci; Loos, Michel; Politi, Mario Jose; Chaimovich, Hernan; Cuccovia, Iolanda Midea
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 5 p. 385 - 397
反应条件
in N,N-dimethyl-formamide
1 h; Heating;
参考文献
Ganin, E. V.; Makarov, V. F.; Nikitin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2209 - 2215
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2415 - 2423
反应条件
1: methanol / 0.25 h / 20 °C
2: sodium hydroxide / water / 24 h / 30 °C
View Scheme
参考文献
De Barros, Teresa Cristina; Filho, Pedro Berci; Loos, Michel; Politi, Mario Jose; Chaimovich, Hernan; Cuccovia, Iolanda Midea
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 5 p. 385 - 397
反应条件
1: methanol / 0.25 h / 20 °C
2: hydrogenchloride / water; dimethyl sulfoxide / 30 °C / aq. buffer
View Scheme
参考文献
De Barros, Teresa Cristina; Filho, Pedro Berci; Loos, Michel; Politi, Mario Jose; Chaimovich, Hernan; Cuccovia, Iolanda Midea
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 5 p. 385 - 397
参考文献
Karischin; Baklan
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3048;engl.Ausg.S.3013
反应条件
1: 62 percent / triethylamine / Ambient temperature
2: 70 percent / amine Vs or Vt / 0.33 h / 200 °C
View Scheme
参考文献
Ganin, E. V.; Makarov, V. F.; Nikitin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2209 - 2215
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2415 - 2423
反应条件
hydrogenchloride in water; dimethyl sulfoxide
T=30°C; aq. buffer; Kinetics; pH-valueTime;
参考文献
De Barros, Teresa Cristina; Filho, Pedro Berci; Loos, Michel; Politi, Mario Jose; Chaimovich, Hernan; Cuccovia, Iolanda Midea
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 5 p. 385 - 397
