N-(二甲基氨基-甲基-硼烷基)-N-甲基-甲胺合成路线 （共 30 条）
反应条件
transamination, boiling the educts under nitrogene, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling of the educts under inert atmosphere, distn. of the dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
参考文献
Noeth, H.; Fritz, P.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 322, p. 297 - 309
Full Text Show Details
Gmelin Handbook: B: B-Verb.4, 3.6, page 66 - 88
参考文献
Noeth, H.; Fritz, P.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 322, p. 297 - 309
Full Text Show Details
Gmelin Handbook: B: B-Verb.4, 3.6, page 66 - 88
反应条件
trimethylamine in diethyl ether
T=-78 - 20°C; Inert atmosphere;
参考文献
Noeth, Heinrich; Taeger, Tilman
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 2 p. 173 - 177
反应条件
in diethyl ether
byproducts: LiCl;
参考文献
Gmelin Handbook: B: B-Verb.4, 9.1, page 268 - 279
参考文献
Noeth,H. et al.
Journal of Organometallic Chemistry, 1964 , vol. 1, p. 401 - 410
反应条件
in diethyl ether
(Ar); Schlenk techniques; Me2NH condensed into Et2O soln. of Me2B2S3 at -78°C; warmed to room temp.; refluxed for 16 h; vac. evapn.; vac. distn.; detn. by NMR;
参考文献
Noeth, Heinrich; Taeger, Tilman
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 2 p. 173 - 177
反应条件
NMe3 in diethyl ether
(Ar); Schlenk techniques; NMe3, Me2NH condensed into Et2O soln. of Me2B2S3 at -78°C; warmed to room temp.; vac. evapn.; vac. distn.; detn. by NMR; elem. anal.;
参考文献
Noeth, Heinrich; Taeger, Tilman
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 2 p. 173 - 177
