1,2-二棕榈酰-3-o-苄基-rac-甘油合成路线 （共 7 条）
反应条件
4-(N,N-dimethlyamino)pyridine
参考文献
Williams, John R.
Steroids, 1995 , vol. 60, # 4 p. 333 - 336
反应条件
zinc(II) chloride
T=20°C; 15 h;
参考文献
Nifantyev, E. E.; Predvoditelev, D. A.; Fursenko, I. V.; Smirnova, L. I.
Synthesis, 1982 , # 2 p. 132 - 134
反应条件
triethylamine in benzene
Acylation; 1 h; Heating;
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
T=0 - 20°C;
参考文献
Martin, Stephen F.; Josey, John A.
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3631 - 3634
反应条件
1: AcOH / propan-2-ol; H2O / 6 h / Heating
2: 30 percent / Py / CHCl3 / 48 h / 20 °C
3: 79 percent / Et3N / benzene / 1 h / Heating
View Scheme
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
反应条件
1: 30 percent / Py / CHCl3 / 48 h / 20 °C
2: 79 percent / Et3N / benzene / 1 h / Heating
View Scheme
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
反应条件
1.1: NaNH2 / benzene / 1 h / Heating
1.2: 57 percent / benzene / 24 h / Heating
2.1: AcOH / propan-2-ol; H2O / 6 h / Heating
3.1: 30 percent / Py / CHCl3 / 48 h / 20 °C
4.1: 79 percent / Et3N / benzene / 1 h / Heating
View Scheme
参考文献
Takahashi, Toshihiro; Ido, Tatsuo; Nagata, Shinji; Iwata, Ren
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 943 - 969
