反应条件
1: 1.) n-BuLi / 1.) hexane, THF, ether, -95 deg C, 30 min, 2.) from -95 deg C to RT, overnight
2: 69 percent / dichlorodimethylsilane, NaI / acetonitrile / 20.5 h
View Scheme
参考文献
Bedard, Thomas C.; Corey, Joyce Y.; Lange, Lura D.; Rath, Nigam P.
Journal of Organometallic Chemistry, 1991 , vol. 401, # 3 p. 261 - 272