iodine 200°C, 5 h, in presence of traces of iodine in autoclave; distn. (90°C, 10 torr), removing of I2 by shaking with Hg, recrystn. from CH3COOH, sublimation (100°C, 1 Torr);
in pentane in a sealed stainless-steel tube at 90-95°C for 14 h;
参考文献
Kobayashi,Y.; Hamana,H.; Fujino,S.
Journal of the American Chemical Society, 1980 , vol. 102, p. 252
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Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.1.2, page 75 - 81
in 1,2,2-trifluoro-trichloroethane 158 h; Ambient temperatureγ-radiation; other alcohols; Product distributionMechanism;
参考文献
Nishida, Masakazu; Hayakawa, Yoshio; Matsui, Masaki; Shibata, Katsuyoshi; Muramatsu, Hiroshige
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 11 p. 3494 - 3496