1,2-二氢-4-甲基-2-氧代-6-苯基-5-嘧啶羧酸乙酯合成路线 （共 8 条）
反应条件
dipotassium peroxodisulfate in water 0.0416667 h; Microwave irradiation;
参考文献
Klingebiel, Uwe; Matthes, Christoph; Ringe, Arne; Magull, Joerg
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 2009 , vol. 64, # 5 p. 532 - 540
反应条件
pyridine hydrochloride 0.5 h; Heating;
参考文献
Vanden Eynde, Jean Jacques; Audiart, Nancy; Canonne, Valerie; Michel, Sophie; Van Haverbeke, Yves; Oliver Kappe
Heterocycles, 1997 , vol. 45, # 10 p. 1967 - 1978
反应条件
1: cerium(III) chloride heptahydrate / methanol / 24 h / Reflux 2: 2-hydroxy-1,3-isoindolinedione; oxygen; [Co(O2CCH3)2]*4H2O / dichloromethane / 1.5 h / 80 °C / 760.05 Torr View Scheme
参考文献
Tetrahedron, , vol. 67, # 31 p. 5615 - 5620
反应条件
1: 60 percent / NaHCO3 / dimethylformamide / 3 h / 70 °C 2: 60 percent / MnO2 / CH2Cl2 / 4 h / Heating 3: 45 percent / pyridinium hydrochloride / 0.5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 45, # 10 p. 1967 - 1978
反应条件
1: 60 percent / NaHCO3 / dimethylformamide / 3 h / 70 °C 2: 60 percent / MnO2 / CH2Cl2 / 4 h / Heating 3: 45 percent / pyridinium hydrochloride / 0.5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 45, # 10 p. 1967 - 1978
反应条件
1: 60 percent / MnO2 / CH2Cl2 / 4 h / Heating 2: 45 percent / pyridinium hydrochloride / 0.5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 45, # 10 p. 1967 - 1978
反应条件
iodine; magnesium in methanol T=50°C; 24 h; chemoselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 19 p. 2219 - 2221
反应条件
iodine; magnesium in methanol T=50°C; 24 h; chemoselective reaction;
参考文献
Singh, Kamaljit; Singh, Kawaljit
Tetrahedron Letters, 2009 , vol. 50, # 19 p. 2219 - 2221
