copper(I) bromide dimethylsulfide complex in diethyl ether
T=-78 - -70°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Heerden, Pieter S. van; Bezuidenhoudt, Barend C. B.; Steenkamp, Jacobus A.; Ferreira, Daneel
Tetrahedron Letters, 1992 , vol. 33, # 17 p. 2383 - 2386
1: 59 percent / diethyl ether / 3 h / 0 °C
2: 65 percent / pyridinium dichromate (PDC) / dimethylformamide / 3 h / 0 °C
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参考文献
Anstead, Gregory M.; Peterson, Chad S.; Pinney, Kevin G.; Wilson, Scott R.; Katzenellenbogen, John A.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 10 p. 2726 - 2734
Eastham; Raaen
Proceedings of the Chemical Society, London, 1958 , p. 149
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Raaen; Eastham
Journal of the American Chemical Society, 1960 , vol. 82, p. 1349,1351