反应条件
1: 2-(dimethoxyphosphoryl)-4,5-dimethyl-2H-1,3-dithiole With potassium tert-butylate in tetrahydrofuran
T=-78°C; Wittig-Horner reaction; 1 h; Inert atmosphere;
2: 2-piperidino-4-methyl-1,3-dithiolium hexafluorophosphate in tetrahydrofuran
T=-78°C; Wittig-Horner reaction; 1 h; Inert atmosphere;
参考文献
Zitouni, Amel; Gouasmia, Abdelkrim; Bouguessa, Sabrina; Kaboub, Lakhemici; Boudiba, Louiza
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 8 p. 1744 - 1754
