3,5-二叔丁基-4-羟基苄醚合成路线 （共 9 条）
反应条件
diammonium succinate in acetone
Ambient temperatureother reagents: ammonium acetate, potassium acetate, ammonium chloride, sodium sulfate; crown ether presence;
参考文献
Bukharov, S. V.; Nusinovich, V. D.; Chugunov, Yu. V.; Efremov, Yu. Ya.; Samuilov, Ya. D.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 2 p. 216 - 217
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 2 p. 244 - 245
反应条件
ammonia in water; acetone
0.5 h; Ambient temperature;
参考文献
Bukharov; Nugumanova; Mukmeneva
Russian Journal of General Chemistry, 1998 , vol. 68, # 10 p. 1605 - 1608
反应条件
perchloric acid; water in acetone
28 h; Heating;
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
perchloric acid in tetrahydrofuran
48 h; Ambient temperature;
参考文献
Davis, Brian R.; Gash, Diana M.; Woodgate, Paul D.; Woodgate, Sheila D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1499 - 1508
反应条件
1: 90 percent / H2O / acetone / 1) 1h, reflux, 2) after addition of water 1h, reflux
2: 41 percent / 72percent HClO4, H2O / acetone / 28 h / Heating
View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
1: 100 percent / acetone / Heating
2: 41 percent / 72percent HClO4, H2O / acetone / 28 h / Heating
View Scheme
参考文献
Nikiforov, G. A.; Bannikov, G. F.; Mal'donado, I. K. A. Romero; Malysheva, R. D.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. <1> 38, # 12 p. 2530 - 2535
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 12 p. 2765 - 2770
反应条件
1: NaBH4 / methanol
2: TsCl, Py
View Scheme
参考文献
Teubner,H.-J. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 757 - 770
反应条件
Nafion H in ethylene glycol dimethyl ether
24 h; Ambient temperature;
参考文献
Davis, Brian R.; Gash, Diana M.; Woodgate, Paul D.; Woodgate, Sheila D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1499 - 1508
反应条件
pyridine; p-toluenesulfonyl chloride
参考文献
Teubner,H.-J. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 757 - 770
