氨基磺酸-2,2,2-三氯乙酯合成路线 (共 9 条)
反应条件
[Rh2(esp)2] in benzene-d6 48 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 21 p. 5827 - 5832
反应条件
[bis(acetoxy)iodo]benzene; C32H44ClN4O4Rh2*3CH2Cl2 Inert atmosphere;
参考文献
Chemical Communications, , vol. 48, # 99 p. 12097 - 12099
反应条件
[bis(acetoxy)iodo]benzene; C32H44ClN4O4Rh2*3CH2Cl2 Inert atmosphere;
参考文献
Kornecki, Katherine P.; Berry, John F.
Chemical Communications, 2012 , vol. 48, # 99 p. 12097 - 12099
反应条件
1: chlorosulphonyl isocyanate With formic acid in acetonitrile
T=23°C; 8 h;
2: 2,2,2-trichloroethyl alcohol in N,N-dimethyl acetamide; acetonitrile
T=23°C; 1.5 h;
参考文献
Fiori, Kristin Williams; Du Bois
Journal of the American Chemical Society, 2007 , vol. 129, # 3 p. 562 - 568
反应条件
amidosulfonyl chloride in N,N-dimethyl acetamide
T=20°C; 24 h;
参考文献
Yamamoto, Hirofumi; Ho, Elisabeth; Sasaki, Ikuo; Mitsutake, Mizuho; Takagi, Yuichi; Imagawa, Hiroshi; Nishizawa, Mugio
European Journal of Organic Chemistry, 2011 , # 13 p. 2417 - 2420
反应条件
in diethyl ether
T=20°C; 0.5 h;
参考文献
Sbihi; Beji; Baklouti
Journal of Fluorine Chemistry, 2002 , vol. 115, # 2 p. 161 - 164
反应条件
in diethyl ether
T=20°C; 1.5 h;
参考文献
Sbihi; Beji; Baklouti
Journal of Fluorine Chemistry, 2002 , vol. 115, # 2 p. 161 - 164
反应条件
C6F13CH(OH)CH2NCH2CH2CH3 in diethyl ether
Heating;
参考文献
Sbihi; Beji; Baklouti
Journal of Fluorine Chemistry, 2002 , vol. 115, # 2 p. 161 - 164
反应条件
in N,N-dimethyl acetamide
T=0 - 20°C; 16 h;
参考文献
Bess, Elizabeth N.; Deluca, Ryan J.; Tindall, Daniel J.; Oderinde, Martins S.; Roizen, Jennifer L.; Du Bois; Sigman, Matthew S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5783 - 5789