反应条件
1: 225 mg / 1.) butyllithium, 2.) Fe(acac)3 / 1.) THF, hexane, 20 min, 2.) THF, hexane, -70 deg C, 2 h 2: 95 percent / NBS / CHCl3; acetic acid / 0.5 h / Heating 3: 1.) TMEDA, butyllithium / 1.) THF, hexane, -80 deg C, 20 min, 2.) THF, hexane, RT, 5 h View Scheme
参考文献
Higuchi, Hiroyuki; Nakayama, Taketoshi; Koyama, Haruki; Ojima, Juro; Wada, Tatsuo; Sasabe, Hiroyuki
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 8 p. 2363 - 2378
