1-叠氮-1-脱氧-Β-D-吡喃乳糖苷合成路线 （共 5 条）
反应条件
sodium methylate in methanol Deacetylation; hydrolysis; pH=9; 2 h;
参考文献
Xue, Jie; Pan, Yanbin; Guo, Zhongwu
Tetrahedron Letters, 2002 , vol. 43, # 9 p. 1599 - 1602
反应条件
sodium azide; DMEG; N-ethyl-N,N-diisopropylamine in water-d2 T=20°C; 0.5 h; stereoselective reaction;
参考文献
Tanaka, Tomonari; Nagai, Hikaru; Noguchi, Masato; Kobayashi, Atsushi; Shoda, Shin-Ichiro
Chemical Communications, 2009 , # 23 p. 3378 - 3379
反应条件
1: 96 percent / NaN3; aq. NaHCO3; Bu4NHSO4 / CH2Cl2 / 2 h / 20 °C 2: 97 percent / NaOMe / methanol / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 50 p. 17618 - 17619
反应条件
1.1: iodotrimethylsilane / CH2Cl2 / 0.5 h / Heating 1.2: 87 percent / tetrabutylammonium azide / CH2Cl2 / 0.17 h 2.1: sodium methoxide / methanol View Scheme
参考文献
Carbohydrate Research, , vol. 338, # 9 p. 835 - 841
反应条件
pyridine T=20°C; 24 h;
参考文献
Erdelyi, Mate; D'Auvergne, Edward; Navarro-Vazquez, Armando; Leonov, Andrei; Griesinger, Christian
Chemistry - A European Journal, 2011 , vol. 17, # 34 p. 9368 - 9376
