4-二乙氨基甲基-2,5-二甲基苯酚合成路线 (共 6 条)
反应条件
sulfur dioxide in acetonitrile
T=20°C; aminomethylation; 42 h;
参考文献
Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1997 , vol. 53, # 39 p. 13361 - 13372
反应条件
1: 66 percent / H2O
2: acetonitrile / 42 h / Ambient temperature; add of SO2
View Scheme
参考文献
Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5801 - 5804
参考文献
Burckhalter et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1894,1896
反应条件
in acetonitrile
T=20°C; aminomethylation; 42 h;
参考文献
Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1997 , vol. 53, # 39 p. 13361 - 13372
反应条件
sulfur dioxide in acetonitrile
42 h; Ambient temperaturewithout SO2; Yield given. Yields of byproduct given;
参考文献
Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5801 - 5804
反应条件
sulfur dioxide in acetonitrile
42 h; Ambient temperaturevar. time and temp; without SO2; Yield given. Yields of byproduct given;
参考文献
Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5801 - 5804