2,5-二甲基-4'-硝基联苯合成路线 (共 5 条)
反应条件
1: With palladium diacetate; silver trifluoroacetate; trifluoroacetic acid in 2,2,2-trifluoroethanol
T=120°C; 2 h; Autoclave;
2: With sodium hydrogencarbonate in 2,2,2-trifluoroethanol
T=120°C; 30 h; Autoclave;
参考文献
Qin, Chunxia; Lu, Wenjun
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7424 - 7427
反应条件
18-crown-6 ether; 10 Pd/C; potassium carbonate in methanol; water
T=45°C; Suzuki-Miyaura Coupling; 2 h;
参考文献
Chu, Wenyi; Li, Xinmin; Hou, Yanjun; Wang, Hua; Li, Hongyu; Yuan, Xiaobin; Sun, Zhizhong
Applied Organometallic Chemistry, 2012 , vol. 26, # 9 p. 478 - 482
反应条件
iso-propyl nitrite; copper(l) chloride
T=20°C; 3 h;
参考文献
Liang, Shuang; Cao, Xiaohui; Yan, Xilong; Chen, Ligong
Journal of Chemical Research, 2012 , vol. 36, # 9 p. 555 - 556
反应条件
potassium acetate; 18-crown-6 ether
1.5 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
ammonium cerium(IV) nitrate in acetonitrile; benzene
24 h; Ambient temperature;
参考文献
Arai, Noriyoshi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 6 p. 1707 - 1714