Johnson; Fritz
Journal of Organic Chemistry, 1954 , vol. 19, p. 74
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.1, page 94 - 98
Alleston, D. L.; Davies, A. G.; Hancock, M.; White, R. F. M.
Journal of the Chemical Society, 1963 , p. 5469 - 5475
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.1, page 94 - 98
in tetrahydrofuran; diethyl ether byproducts: CH3SCH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 12d; not isolated; monitored by (119)Sn NMR spectra; < 5percent conversion;
in tetrahydrofuran; diethyl ether byproducts: C6H5SCH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 9 d; not isolated; monitored by (119)Sn NMR spectra; < 10percent conversion;
in tetrahydrofuran; diethyl ether byproducts: C6H5S(O)2CH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 1 h; not isolated; monitored by (119)Sn NMR spectra; 90-95percent conversion;
in tetrahydrofuran; diethyl ether byproducts: CH3S(O)2CH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 1 h; not isolated; monitored by (119)Sn NMR spectra; 80-95percent conversion;
