反应条件
in diethyl ether; pentane
byproducts: butane, MgBrI; (inert atmosphere); slow dropwise addn. of excess of Et2NH to soln. of BuMgBr in ether (-10°C), pptn., warming to room temp., refluxing (20 min), cooling to -15°C, dropwise addn. of Sn-compd. in pentane, heating (1 h), standing (overnight); decanting (under Ar), solvent evapn., distn. (vac.); elem. anal.;
参考文献
Nikitin, N. S.; Zavgorodnii, V. S.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1027 - 1031
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1147 - 1152
