反应条件
hydrogenchloride in methanol; diethyl ether; water
Mg compd. added to soln. of B compd. at -65--70°C dropwise within1.5 h, warmed to 20°C within 3 h, hydrolysed with aq. HCl, org. phase sepd., aq. phase extd. with ether, dried with MgSO4, dissolved in MeOH, reacted with aq. B compd.; after 5 min filtered, dried, extd. with hot acetone, solvent removed in vac., dried over P4O10, elem. anal.;
参考文献
Bardin; Idemskaya; Frohn
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 4 p. 883 - 890
