1: cyclohexanecarboxylic acid ethyl ester With LDBBA in tetrahydrofuran; hexane
T=0°C;
2: n-butyl-magnesium chloride in tetrahydrofuran; diethyl ether; hexane
T=20°C;
3: With hydrogenchloride; water in tetrahydrofuran; diethyl ether; hexane
参考文献
Chae, Min Jung; Jeon, Ah Ram; Park, Jae Kyo; An, Duk Keun
Tetrahedron Letters, 2011 , vol. 52, # 14 p. 1718 - 1720
Rasmussen; Brattain; Zucco
Journal of Chemical Physics, 1947 , vol. 15, p. 136,140 Anm.
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Cleveland
Journal of Chemical Physics, 1943 , vol. 11, p. 4