N,N'-二异丙基碳二亚胺合成路线 (共 71 条)
反应条件
in chloroform T=120°C;
参考文献
Richter, R.; Stuber, F. A.; Tucker, B.
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3675 - 3681
反应条件
1: toluene / 0.75 h / Ambient temperature 2: 93 percent / 20percent HCl / ethanol / 12 h / Ambient temperature View Scheme
参考文献
Katagiri, Nobuya; Morishita, Yoshihiro; Kaneko, Chikara
Heterocycles, 1997 , vol. 46, # 1 p. 503 - 508
反应条件
in dichloromethane 34 h; Irradiation;
参考文献
Lwowski, Walter; Kanemasa, Suji; Murray, Roy A.; Ramakrishnan, V. T.; Thiruvengadam, T. K.; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 10 p. 1719 - 1723
反应条件
2-mercaptopropanoic acid in benzene
参考文献
Monforte,P. et al.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 341 - 345
反应条件
copper(l) chloride T=25°C; 15 h;
参考文献
Collingwood, Stephen P; Davies, Alan P; Golding, Bernard T
Tetrahedron Letters, 1987 , vol. 28, # 38 p. 4445 - 4448
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Lochte; Noyes; Bailey
Journal of the American Chemical Society, 1922 , vol. 44, p. 2561
反应条件
hydroxylamine in 1,4-dioxane
Ambient temperature;
参考文献
Zinner,G.; Gross,H.
Chemische Berichte, 1972 , vol. 105, p. 1709 - 1713
反应条件
(i) AcCl, CH2Cl2, (ii) /BRN= 2621160/, (iii) Et3N; Multistep reaction;
参考文献
Hartke,K.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1967 , vol. 300, # 9 p. 766 - 772
反应条件
1: With Sm[N(TMS)2]2(THF)3 in tetrahydrofuran; hexane
T=-10 - 20°C; Inert atmosphere;
2: With aniline in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
3: With water in tetrahydrofuran
Inert atmosphere;
参考文献
Du, Zhu; Li, Wenbo; Zhu, Xuehua; Xu, Fan; Shen, Qi
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8966 - 8972
反应条件
sodium hydride in tetrahydrofuran
4 h;
参考文献
Richter, Monika; Strauss, Karin; Augustin, Manfred
Zeitschrift fuer Chemie (Stuttgart, Germany), 1982 , vol. 22, # 3 p. 103 - 104