N,N'-二异丙基碳二亚胺合成路线 （共 71 条）
反应条件
sodium hydride in tetrahydrofuran
4 h;
参考文献
Richter, Monika; Strauss, Karin; Augustin, Manfred
Zeitschrift fuer Chemie (Stuttgart, Germany), 1982 , vol. 22, # 3 p. 103 - 104
反应条件
alkali hydroxide
T=25°C;
参考文献
Lochte; Noyes; Bailey
Journal of the American Chemical Society, 1922 , vol. 44, p. 2561
反应条件
trimethylsilylacetylene in benzene
T=50 - 60°C; 48 h;
参考文献
Tsuge, Otohiko; Urano, Satoshi; Oe, Koji
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5130 - 5136
反应条件
[σ:η1:η5-(OCH2)(Me2NCH2)C2B9H9]Ti-(NMe2) in toluene
T=115°C; 168 h;
参考文献
Shen, Hao; Wang, Yang; Xie, Zuowei
Organic Letters, 2011 , vol. 13, # 17 p. 4562 - 4565
反应条件
1: 1) neat, 100 deg C, 20 h; 2) isopropyl alcohol
2: 90.1 percent Chromat. / KOH, KCl / H2O; ethanol / 25 °C / δH(excit.); δS(excit.)
View Scheme
参考文献
Suttle, Nicola A.; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1369 - 1372
参考文献
Benoiton, N. Leo; Chen, Francis M. F.
Journal of the Chemical Society, Chemical Communications, 1981 , # 23 p. 1225 - 1227
反应条件
in pentane
adding a stoichiometric amt. of dicyclohexylcarbodiimide to a soln. of the W complex (20°C), reacting (24 h); column chromy. (silica gel), eluting the isocyanide complex (pentane), eluting the Schiff base (ether);
参考文献
Weiss, Karin; Kindl, Petra
Angewandte Chemie, 1984 , vol. 96, # 8 p. 616 - 617
参考文献
Kollenz, Gert; Penn, Gerhard; Ott, Walter; Peters, Karl; Peters, Eva-Maria; et al.
Chemische Berichte, 1984 , vol. 117, # 4 p. 1310 - 1329
反应条件
1,2,3,4-tetramethyl benzene; ortho-vanadic acid tert-butylester in para-xylene
T=138°C; catalytic metathesis; 25 h; Product distributionKinetics; Further Variations:Catalysts;
参考文献
Birdwhistell; Lanza; Pasos
Journal of Organometallic Chemistry, 1999 , vol. 584, # 1 p. 200 - 205
反应条件
in tetrahydrofuran
inert atmosphere; 2 equiv. diimide, room temp.; concn. (vac.), crystn. (-30°C, overnight), repeated recrystn. (THF); elem. anal.;
参考文献
Dionne, Michel; Hao, Shoukang; Gambarotta, Sandro
Canadian Journal of Chemistry, 1995 , vol. 73, # 7 p. 1126 - 1134
