1.1: thionyl chloride / 2 h / Reflux
2.1: benzene / 1 h / Cooling with ice; Reflux
3.1: sodium tetrahydroborate; ethanol / 1.5 h / 20 °C
4.1: potassium hydroxide / ethanol; water / 4.5 h / Reflux
4.2: pH 7
View Scheme
参考文献
Abraham, Shibu; Lan, Yaqi; Lam, Ricky S. H.; Grahame, Douglas A. S.; Kim, Jennifer Jae Hee; Weiss, Richard G.; Rogers, Michael A.
Langmuir, 2012 , vol. 28, # 11 p. 4955 - 4964
