3,3-二氟-3H-双吖丙啶合成路线 （共 12 条）
参考文献
Mitsch,R.A.; Robertson,J.E.
Journal of Heterocyclic Chemistry, 1965 , vol. 2, p. 152 - 156
参考文献
Mitsch,R.A.; Robertson,J.E.
Journal of Heterocyclic Chemistry, 1965 , vol. 2, p. 152 - 156
反应条件
oxygen T=24.9°C; P=750.06 Torr; Irradiationother temperature; dependence on wavelength; Product distributionMechanism;
参考文献
Angewandte Chemie, , vol. 106, # 10 p. 1161 - 1163
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; 15-crown-5; LiF in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=55°C; P=1 Torr; Molecular sieveCooling with liquid nitrogen;
参考文献
Moss, Robert A.; Wang, Lei; Krogh-Jespersen, Karsten
Journal of the American Chemical Society, 2009 , vol. 131, p. 2128 - 2130
反应条件
sodium perchlorate in acetonitrile
Electrochem. Process; by cathodic reduction;
参考文献
Rebertus; Toren
Journal of Organic Chemistry, 1967 , vol. 32, p. 4045
反应条件
water
byproducts: {(C4H9)4N}F, OCN(1-); yield of F2CNN depends on the water content; further by-products;
参考文献
Rebertus,R.L. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1944 - 1947
反应条件
cesium fluoride
24°C;
参考文献
Meyers; Frank
Inorganic Chemistry, 1966 , vol. 5, p. 1455
反应条件
Electrochem. Process; by cathodic reduction;
参考文献
Rebertus; Toren
Journal of Organic Chemistry, 1967 , vol. 32, p. 4045
反应条件
Irradiation (UV/VIS); molar ratio of difluoro diazirine:NO2=1:5; UV-photolysis at 20°C 16-20 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
反应条件
Irradiation (UV/VIS); molar ratio of difluoro diazirine:NO2=1:5; UV-photolysis at 20°C 16-20 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
