1,3二氯-1,1,3,3-四异丙基二硅氧烷合成路线 （共 9 条）
反应条件
acetyl chloride; palladium on activated charcoal 30 h; Ambient temperature;
参考文献
Zhang, H. X.; Guibe, F.; Balavoine, G.
Synthetic Communications, 1987 , vol. 17, # 11 p. 1299 - 1308
反应条件
1: 85 percent / P2O5 2: 78 percent / Cl2 / CCl4 / 0.5 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 12 p. 4059 - 4065
参考文献
Wacker-Chemie GmbH
Patent: US6284907 B1, 2001 ;
参考文献
Wacker-Chemie GmbH
Patent: US6284907 B1, 2001 ;
参考文献
Honda, Sinkichi; Terada, Kazunori; Sato, Yoshinobu; Sekine, Mitsuo; Hata, Tsujiaki
Chemistry Letters, 1982 , p. 15 - 18
反应条件
1: 89 percent / pyridine / 12 h 2: 50 percent / 4-(dimethylamino)pyridine / acetonitrile / 12 h / 24 °C 3: 65 percent / tributyltin hydride, azobisisobutyronitrile / toluene / 3 h / Heating View Scheme
参考文献
Khazanchi; Yu; Johnson
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2552 - 2556
反应条件
1: 89 percent / pyridine / 12 h 2: 50 percent / 4-(dimethylamino)pyridine / acetonitrile / 12 h / 24 °C View Scheme
参考文献
Khazanchi; Yu; Johnson
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2552 - 2556
反应条件
1: 97 percent / pyridine / 4 h / Ambient temperature
2: 69 percent / dimethylformamide / 4 h / Ambient temperature
View Scheme
参考文献
Pankiewicz, Krzysztof; Matsuda, Akira; Watanabe, Kyoichi A.
Journal of Organic Chemistry, 1982 , vol. 47, # 3 p. 485 - 488
参考文献
Weinberg, Jennifer M.; Wooley, Karen L.
Journal of Organometallic Chemistry, 1997 , vol. 542, # 2 p. 235 - 240
