3,4-二乙基-3,4-己烷二醇合成路线 （共 16 条）
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in trifluoroacetic acid T=30°C; 0.1 h;
参考文献
Moorthy, Jarugu Narasimha; Singhal, Nidhi; Senapati, Kalyan
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 5 p. 767 - 771
反应条件
1: orthophosphoric acid 2: hydroquinone; picric acid / 180 °C 3: phosphorus (V)-oxide View Scheme
参考文献
Skwartschenko et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2605,2608; engl. Ausg. S. 2569, 2571
反应条件
sodium hydride in tetrahydrofuran T=50°C; 14 h;
参考文献
Dogan, Barbara; Beckhaus, Hans-Dieter; Birkhofer, Hermann; Ruechardt, Christoph
Chemische Berichte, 1990 , vol. 123, # 6 p. 1365 - 1368
反应条件
1: cerium; Monobrombernsteinsaeuraethylester (germ.)=monobromo ethyl succinate With iodine in tetrahydrofuran
T=0°C; 0.5 h; Inert atmosphere;
2: pentan-3-one in tetrahydrofuran
T=0 - 20°C; 3.5 h; Inert atmosphere;
参考文献
Rodrigues, Shirley M. M.; Nardini, Viviani; Constantino, Mauricio G.; Da Silva, Gil Valdo J.
Tetrahedron Letters, 2012 , vol. 53, # 45 p. 6136 - 6137,2
反应条件
aluminum-mercury amalgam in benzene
14 h; Heating;
参考文献
Birkhofer, Hermann; Beckhaus, Hans-Dieter; Ruechardt, Christoph
Chemische Berichte, 1993 , vol. 126, # 4 p. 1023 - 1030
反应条件
cerium; iodine in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Sumimoto, Norifumi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of Organic Chemistry, 1990 , vol. 55, # 5 p. 1628 - 1631
反应条件
cerium; iodine in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Sumimoto, Norifumi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of Organic Chemistry, 1990 , vol. 55, # 5 p. 1628 - 1631
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; Reformatsky type reaction; 2 h; Inert atmosphere;
参考文献
Nagano, Takao; Motoyoshiya, Jiro; Kakehi, Akikazu; Nishii, Yoshinori
Organic Letters, 2008 , vol. 10, # 23 p. 5453 - 5456
反应条件
Mg-graphite in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Csuk, Rene; Fuerstner, Alois; Weidmann, Hans
Journal of the Chemical Society, Chemical Communications, 1986 , # 24 p. 1802 - 1803
反应条件
titanium tetrachloride; lithium in tetrahydrofuran
T=20°C; 10 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Villiers, Claude; Ephritikhine, Michel
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 21 p. 2380 - 2382
