3,4-二乙基-3,4-己烷二醇合成路线 （共 16 条）
反应条件
titanium tetrachloride; lithium in tetrahydrofuran
T=20°C; 10 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Villiers, Claude; Ephritikhine, Michel
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 21 p. 2380 - 2382
反应条件
titanium tetrachloride; magnesium; ethylene dibromide
1.) benzene, 0 deg C, 30 min, 2.) 5-10 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rao, S. Achyutha; Periasamy, M.
Tetrahedron Letters, 1988 , vol. 29, # 13 p. 1583 - 1586
反应条件
titanium tetrachloride; magnesium
1.) benzene, 0 deg C, 30 min, 2.) 5-10 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rao, S. Achyutha; Periasamy, M.
Tetrahedron Letters, 1988 , vol. 29, # 13 p. 1583 - 1586
反应条件
titanium(III) chloride
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Dams, R.; Malinowski, M.; Geise, H. J.
Bulletin des Societes Chimiques Belges, 1982 , vol. 91, # 4 p. 311 - 320
反应条件
hexacarbonyl molybdenum in diethyl ether
2 h; var. catalysts; Product distribution;
参考文献
Sobota, Piotr; Kaczurba, Eleonora
Journal of Organometallic Chemistry, 1982 , vol. 235, # 3 p. 295 - 300
反应条件
1: sulfuric acid
2: nitric acid
View Scheme
参考文献
Meerwein
Justus Liebigs Annalen der Chemie, 1919 , vol. 419, p. 165
