diethyl ether; benzyl-magnesium bromide
Erhitzen des von Aether befreiten Reaktionsgemisches mit Xylol;
参考文献
Starr et al.
Journal of the American Chemical Society, 1932 , vol. 54, p. 3971,3974
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Craig; Bulbrook; Hixon
Journal of the American Chemical Society, 1931 , vol. 53, p. 1833
1: acetyl chloride With pyridine in dichloromethane
T=20°C; 0.25 h;
2: 2-benzyl-Δ1-pyrroline in dichloromethane
T=20°C; 3 h;
3: With hydrogenchloride in dichloromethane
参考文献
Zakurdaev, Eugene P.; Balenkova, Elizabeth S.; Nenajdenko, Valentine G.
Mendeleev Communications, 2006 , # 4 p. 213 - 215
Quinto, Tommaso; Schwizer, Fabian; Zimbron, Jeremy M.; Morina, Albert; Koehler, Valentin; Ward, Thomas R.
ChemCatChem, 2014 , vol. 6, # 4 p. 1010 - 1014