钝叶扁柏氨基甲酸酯 A; 4-甲基苯-1,3-二氨基甲酸二甲酯合成路线 （共 25 条）
反应条件
[emim][PF6] T=200 - 240°C; P=48.7549 Torr; 2.16667 h;
参考文献
LANZHOU INSTITUTE OF CHEMICAL PHYSICS, CHINESE ACADEMY OF SCIENCES
Patent: US2011/21810 A1, 2011 ;
Location in patent: Page/Page column 5 ;
反应条件
montmorillonite K-10 in decalin T=190°C; 24 h;
参考文献
Uriz, Pedro; Serra, Marc; Salagre, Pilar; Castillon, Sergio; Claver, Carmen; Fernandez, Elena
Tetrahedron Letters, 2002 , vol. 43, # 9 p. 1673 - 1676
反应条件
[2,2']bipyridinyl; tri-ruthenium(0)dodecacarbonyl; montmorillonitebipyridynylpalladium(II) acetate (Pd-clay) in benzene
T=180°C; P=53200 Torr; 24 h;
参考文献
Valli, V. L. K.; Alper, Howard
Journal of the American Chemical Society, 1993 , vol. 115, # 9 p. 3778 - 3779
反应条件
Zn4O(OAc)6
T=190°C; 3 h; AutoclaveInert atmosphere;
参考文献
Bayer MaterialScience AG
Patent: EP2230228 A1, 2010 ;
Location in patent: Page/Page column 8; 9 ;
反应条件
hydrogen; Au/CeO2
T=150°C; P=11251.1 Torr; 23 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Consejo Superior de Investigaciones Cientificas (CSIC); Universidad Politécnica De Valencia (UPV) (50percent)
Patent: EP2407449 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
1,10-phenanthroline; C14H29(C6H13)3P(+)PF6(-); palladium dichloride
T=135°C; P=10343.2 Torr; 24 h;
参考文献
Yang, Qian; Robertson, Al; Alper, Howard
Organic Letters, 2008 , vol. 10, # 21 p. 5079 - 5082
反应条件
tetraethylammonium chloride; tri-ruthenium(0)dodecacarbonyl in toluene
T=160 - 170°C; P=82 Torr; 5 h;
参考文献
Cenini, Sergio; Pizzotti, Maddalena; Crotti, Corrado; Porta, Francesca; Monica, Girolamo La
Journal of the Chemical Society, Chemical Communications, 1984 , # 19 p. 1286 - 1287
反应条件
Pd(1,3-bis(diphenylphosphino)-propane)Cl2; potassium carbonate in benzene
T=155 - 160°C; P=15514.4 Torr; 50 h;
参考文献
Reddy, Nagavelli P.; Masdeu, Anna M.; Ali, Bassam El; Alper, Howard
Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 863 - 864
反应条件
Pd(phen)2(OTf)2; 2-chloro-5-carboxybenzene in chlorobenzene
T=135°C; P=45003.6 Torr; 2 h; Yield given. Yields of byproduct given;
参考文献
Wehman, Petra; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemical Communications, 1996 , # 2 p. 217 - 218
反应条件
oxygen; triphenylphosphine; AuCl(PPh3)2
T=200°C; P=37503.8 Torr; 3 h;
参考文献
Shi; Deng
Chemical Communications, 2001 , # 5 p. 443 - 444
