钝叶扁柏氨基甲酸酯 A; 4-甲基苯-1,3-二氨基甲酸二甲酯合成路线 (共 25 条)
反应条件
Pd(phen)2(OTf)2 in chlorobenzene
T=135°C; P=45003.6 Torr; 2 h; Yield given;
参考文献
Wehman, Petra; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemical Communications, 1996 , # 2 p. 217 - 218
反应条件
N,N'-disalicylidene-1,2-phenylenediiminatocobalt(II); toluene-4-sulfonic acid
T=170 - 200°C; P=37503.8 Torr; 6.08333 h;
参考文献
PHILIPPS-UNIVERSITAeT MARBURG
Patent: WO2006/131381 A1, 2006 ;
Location in patent: Page/Page column 20 ;
反应条件
Fe/CeO2
8 h; vial which can withstand pressure; Product distribution / selectivity;
参考文献
Consejo Superior De Investigaciones Científicas; Universidad Politecnica De Valencia
Patent: EP2316822 A1, 2011 ;
Location in patent: Page/Page column 7-8 ;
反应条件
PbAl2O4 on alumina
T=160°C; P=6965.99 Torr; Product distribution / selectivity;
参考文献
Molzahn, David C.
Patent: US2008/227999 A1, 2008 ;
Location in patent: Page/Page column 4; 6; 7; 9 ;
反应条件
in methanol
T=160°C; 4 h; Inert atmosphereAutoclave; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: US2010/298592 A1, 2010 ;
Location in patent: Page/Page column 8 ;
参考文献
Wang, Qiong; Stidham, Howard D.; Papadimitrakopolos, F.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1994 , vol. 50, # 3 p. 421 - 434
反应条件
gold on nanocrystalline ceria; hydrogen
T=150°C; P=3750.38 Torr; 12 h; chemoselective reaction;
参考文献
Juarez, Raquel; Concepcion, Patricia; Corma, Avelino; Fornes, Vicente; Garcia, Hermenegildo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 7 p. 1286 - 1290
反应条件
phenyl-phosphonic acid; 2,2-dimethoxy-propane; 2-Methyl-5-nitro-phenylamine; {Pd([1,10]phenanthroline)2}[BF4]2
T=150°C; P=45003.6 Torr; 5 h; Product distributionKinetics; Further Variations:ReagentsTemperaturesPressuresCatalysts;
参考文献
Gasperini, Michela; Ragaini, Fabio; Cazzaniga, Chiara; Cenini, Sergio
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 1 p. 105 - 120
反应条件
zinc diacetate; hydrogen
T=140°C; P=3750.38 Torr;
参考文献
Juarez, Raquel; Concepcion, Patricia; Corma, Avelino; Fornes, Vicente; Garcia, Hermenegildo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 7 p. 1286 - 1290
反应条件
1: pyridine; petroleum ether
2: pyridine; petroleum ether
View Scheme
参考文献
Parker et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 594