2-(2-碘苯基)-2-丙醇合成路线 （共 23 条）
反应条件
1: deuterium oxide / cyclohexane / 0.5 h / ultrasound 2: di-tert-butylperoxyoxalate / 2 h / Heating View Scheme
参考文献
Dolenc, Darko; Plesnicar, Bozo
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2628 - 2632
反应条件
(tBuOOCO)2 deiodination; 2 h; Heating;
参考文献
Dolenc, Darko; Plesnicar, Bozo
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2628 - 2632
反应条件
dibenzoyl peroxide deiodination; 24 h; Heating;
参考文献
Dolenc, Darko; Plesnicar, Bozo
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2628 - 2632
反应条件
caesium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; 24 h;
参考文献
Iwasaki, Masayuki; Iino, Shohei; Nishihara, Yasushi
Organic Letters, 2013 , vol. 15, # 20 p. 5326 - 5329
反应条件
1: tBuOCl 2: 100 percent / acetonitrile / 15 h / 20 °C 3: 46 percent / CsF / acetonitrile / 16 h / 20 °C View Scheme
参考文献
Matousek, Vaclav; Pietrasiak, Ewa; Schwenk, Rino; Togni, Antonio
Journal of Organic Chemistry, 2013 , vol. 78, # 13 p. 6763 - 6768
反应条件
(tBuOOCO)2 deiodination; 2 h; Heating;
参考文献
Dolenc, Darko; Plesnicar, Bozo
Journal of the American Chemical Society, 1997 , vol. 119, # 11 p. 2628 - 2632
反应条件
pyridine; palladium diacetate in N,N-dimethyl-formamide T=120°C; 2 h;
参考文献
Kadnikov, Dmitry V.; Larock, Richard C.
Mendeleev Communications, 2007 , vol. 17, # 2 p. 74 - 76
反应条件
in diethyl ether
1 h; Heating;
参考文献
Moss, Robert A.; Wilk, Boguslawa; Krogh-Jespersen, Karsten; Blair, John T.; Westbrook, John D.
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 250 - 258
反应条件
acetic acid; triphenylphosphine in dichloromethane
T=23°C; 0.0833333 h;
参考文献
Powers, David C.; Lee, Eunsung; Ariafard, Alireza; Sanford, Melanie S.; Yates, Brian F.; Canty, Allan J.; Ritter, Tobias
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12002 - 12009
反应条件
MeMgBr in hexane; ethyl acetate; toluene
参考文献
Merck Frosst Canada, Inc.
Patent: US5270324 A1, 1993 ;
