2,6-二甲基吡啶-3-硼酸频那醇酯合成路线 (共 1 条)
反应条件
1: 3-bromo-2,6-dimethylpyridine With n-butyllithium in diethyl ether; hexane
T=-78°C; 0.75 h;
2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in diethyl ether; hexane
T=-78°C; 3 h;
参考文献
Cowart, Marlon D.; Sun, Minghua; Zhao, Chen; Zheng, Guo Zhu
Patent: US2007/66588 A1, 2007 ;
Location in patent: Page/Page column 29-30 ;
US 20070066588 A1