癸烷-1,2,9,10-四醇合成路线 （共 3 条）
反应条件
1: D-(-)-diethyltartrate, titanium tetraisopropoxide, molecular sieves 4A, tert-butylhydroperoxide / CH2Cl2 / 3 h / -20 °C
2: 2.3 mg / H2 / PtO2 / ethanol / 1 h / Ambient temperature
View Scheme
参考文献
Takahashi; Endo; Nozoe
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 12 p. 3181 - 3184
反应条件
1: 78.6 percent / DIBAH / hexane; benzene / 1 h / 0 °C
2: D-(-)-diethyltartrate, titanium tetraisopropoxide, molecular sieves 4A, tert-butylhydroperoxide / CH2Cl2 / 3 h / -20 °C
3: 2.3 mg / H2 / PtO2 / ethanol / 1 h / Ambient temperature
View Scheme
参考文献
Takahashi; Endo; Nozoe
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 12 p. 3181 - 3184
参考文献
Golding,B.T. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1978 , p. 839 - 848
