四氢-2H-吡喃-2-醇合成路线 （共 136 条）
反应条件
in benzene
T=90°C; Wittig reaction; 1.5 h;
参考文献
Bull, James A.; Charette, Andre B.
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1895 - 1902
参考文献
Akita; Yamada; Matsukura; Nakata; Oishi
Tetrahedron Letters, 1990 , vol. 31, # 12 p. 1731 - 1734
反应条件
sodium hydride
1.) dioxane, 5 deg C, 2.) dioxane, 25 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Passarotti; Valenti; Ceriani; Grianti
Bollettino Chimico Farmaceutico, 1993 , vol. 132, # 5 p. 150 - 152
反应条件
1: tetrahydrofuran / -78 deg C, up to rt
2: CrO3
View Scheme
参考文献
Posner, Gary H.; Crouch, R. David; Kinter, Chris M.; Carry, Jean-Christophe
Journal of Organic Chemistry, 1991 , vol. 56, # 25 p. 6981 - 6987
反应条件
1: 2) CrO3, H2SO4 / 1) benzene, 25 deg C
2: iBu2AlH / CH2Cl2 / -78 °C
View Scheme
参考文献
Nicolaou, Kyriacos C.; Petasis, Nicos A.; Seitz, Steven P.
Journal of the Chemical Society, Chemical Communications, 1981 , # 22 p. 1195 - 1196
反应条件
1: tetrahydrofuran / 60 °C
2: (COCl)2; DMSO; Et3N
View Scheme
参考文献
Restrepo-Sanchez, Nora E.; Gomez, Fernando J.; Jaramillo-Gomez, Luz M.; Hudlicky, Tomas
Synthetic Communications, 1999 , vol. 29, # 16 p. 2795 - 2806
反应条件
1: tetrahydrofuran / 0 °C
2: PDC, HOAc, 4-A sieves / CH2Cl2
View Scheme
参考文献
Enholm, Eric J.; Kinter, Kevin S.
Journal of the American Chemical Society, 1991 , vol. 113, # 20 p. 7784 - 7785
反应条件
chromium(VI) oxide; sulfuric acid
1) benzene, 25 deg C; Yield given. Multistep reaction;
参考文献
Nicolaou, Kyriacos C.; Petasis, Nicos A.; Seitz, Steven P.
Journal of the Chemical Society, Chemical Communications, 1981 , # 22 p. 1195 - 1196
反应条件
in tetrahydrofuran; toluene
参考文献
O'Hanlon, Peter J.; Rogers, Norman H.; Tyler, John W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2655 - 2657
反应条件
1: 0.346 g / toluene; tetrahydrofuran
2: 1.) diphenyl disulphide, 2.) thionyl chloride / 1.) irradiation, benzene, 42 h, 2.) reflux, 4 h, 3.) RT, overnight
View Scheme
参考文献
O'Hanlon, Peter J.; Rogers, Norman H.; Tyler, John W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2655 - 2657
