四氢-2H-吡喃-2-醇合成路线 （共 136 条）
反应条件
pyridine-2-carboxylic acid; [Mn(ClO4)2]*6H2O; dihydrogen peroxide; sodium acetate in acetonitrile T=0 - 20°C;
参考文献
ChemSusChem, , vol. 6, # 9 p. 1774 - 1778
反应条件
Re2O7 in dichloromethane T=20°C; 1 h;
参考文献
Sittiwong, Wantanee; Richardson, Michael W.; Schiaffo, Charles E.; Fisher, Thomas J.; Dussault, Patrick H.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1526 - 1532
反应条件
1: 1H-imidazole / tetrahydrofuran / |Inert atmosphere 2: Re2O7 / dichloromethane / 1 h / 20 °C View Scheme
参考文献
Sittiwong, Wantanee; Richardson, Michael W.; Schiaffo, Charles E.; Fisher, Thomas J.; Dussault, Patrick H.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1526 - 1532
反应条件
1: potassium carbonate View Scheme
参考文献
Glacet
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 234, p. 635
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; Mitsunobu reaction; 2 h;
参考文献
Azzouz, Rabah; Bischoff, Laurent; Fouquet, Marc-Henri; Marsais, Francis
Synlett, 2005 , # 18 art. no. D17805ST, p. 2808 - 2810
反应条件
carbon tetrabromide; triphenylphosphine T=20°C; 16 h;
参考文献
Schmalisch, Sebastian; Mahrwald, Rainer
Organic Letters, 2013 , vol. 15, # 22 p. 5854 - 5857
反应条件
Re2O7 in dichloromethane T=20°C; Inert atmosphere; Time;
参考文献
Sittiwong, Wantanee; Richardson, Michael W.; Schiaffo, Charles E.; Fisher, Thomas J.; Dussault, Patrick H.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1526 - 1532
反应条件
2: pyridinium chlorochromate View Scheme
参考文献
Bestmann; Li
Tetrahedron Letters, 1981 , vol. 22, # 49 p. 4941 - 4944
参考文献
Booth, Harold; Kheidhair, Kheidhair A.; Readshaw, Simon A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4699 - 4724
反应条件
1: 73.1 percent / hexane; tetrahydrofuran / 0.75 h / 0 °C 2: 83.6 percent / pyridinium dichromate / dimethylformamide / 4 h / Ambient temperature View Scheme
参考文献
Takano, Seiichi; Chiba, Hiroyuki; Kudo, Junko; Takahashi, Michiyasu; Ogasawara, Kunio
Heterocycles, 1987 , vol. 26, # 9 p. 2461 - 2468
