in benzene
byproducts: Co4(CO)12, CO, C5H5N; under inert atm.; soln. of complex and C5H5NO maintained at 60°C for a few min; filtered under Ar, concd.; not isolated; 1H-NMR;
参考文献
Barrau, Jacques; Hamida, Najib Ben
New Journal of Chemistry, 1991 , vol. 15, p. 657 - 664
1: With potassium tert-butylate in N,N-dimethyl-formamide
T=-20°C; 0.5 h; Inert atmosphere;
2: With acetic acid in N,N-dimethyl-formamide
T=-20°C; Inert atmosphere;
参考文献
Prokhorov, Anton M.; Makosza, Mieczyslaw; Chupakhin, Oleg N.
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1444 - 1446
(AuC2Ph)n; benzoyl chloride in hexane
T=70°C; 1 h; further acetylides; further solvents; variation of reaction time and temperature; Product distribution;
