1: 1-bromo-2-chloro-benzene; 2-methoxy-phenylmagnesium bromide With magnesium in tetrahydrofuran T=60°C; 2.5 h; 2: chloro-dicyclohexylphosphine With copper(l) chloride in tetrahydrofuran T=20°C; 16 h; Further stages.;
参考文献
Parrish; Buchwald
Journal of Organic Chemistry, 2001 , vol. 66, # 11 p. 3820 - 3827
1: 2-Bromo-N,N-dimethylaniline With magnesium in tetrahydrofuran Heating; 2: 1-bromo-2-chloro-benzene in tetrahydrofuran T=60°C; 2.25 h; 3: chloro-dicyclohexylphosphine With copper(l) chloride in tetrahydrofuran; diethyl ether T=20°C; 1 h; Further stages.;
参考文献
Kaye, Steven; Fox, Joseph M.; Hicks, Frederick A.; Buchwald, Stephen L.
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 8 p. 789 - 794