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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴氯苯
合成路线
（共 250 条）
108-86-1
溴代苯
+
694-80-4
2-溴氯苯
→
反应条件
644-08-6
4-甲基联苯
+
19493-33-5
2-氯-4'-甲基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 72 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
694-80-4
2-溴氯苯
+
108-44-1
3-甲基苯胺
→
反应条件
3652-91-3
2-甲基咔唑
反应条件
potassium phosphate; palladium diacetate; tri-cyclo-hexyl-phosphine in 1-methyl-pyrrolidin-2-one T=130°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Ackermann, Lutz; Althammer, Andreas; Mayer, Peter
Synthesis, 2009 , # 20 p. 3493 - 3503
694-80-4
2-溴氯苯
+
104-94-9
对甲氧基苯胺
→
反应条件
18992-85-3
反应条件
potassium phosphate; palladium diacetate; tri-cyclo-hexyl-phosphine in 1-methyl-pyrrolidin-2-one T=130°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Ackermann, Lutz; Althammer, Andreas; Mayer, Peter
Synthesis, 2009 , # 20 p. 3493 - 3503
872-10-6
+
694-80-4
2-溴氯苯
→
反应条件
1129-70-0
反应条件
(i) nBuLi, Et2O, (ii) aq. HClO4; Multistep reaction;
参考文献
Franzen,V. et al.
Justus Liebigs Annalen der Chemie, 1962 , vol. 654, p. 82 - 91
694-80-4
2-溴氯苯
→
反应条件
13130-19-3
反应条件
1: base / Pd2(dba)3; ligand / dioxane / Heating 2: 94 percent / NaHMDS / Pd2(dba)3; DPEphos / toluene / 100 °C View Scheme
参考文献
Willis, Michael C.; Taylor, Dawn; Gillmore, Adam T.
Organic Letters, 2004 , vol. 6, # 25 p. 4755 - 4757
694-80-4
2-溴氯苯
+
57-13-6
→
反应条件
13208-19-0
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine) in 1,4-dioxane T=100°C; 5 h;
参考文献
Sergeev, Alexey G.; Artamkina, Galina A.; Beletskaya, Irina P.
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4719 - 4723
694-80-4
2-溴氯苯
+
57-13-6
→
反应条件
13208-19-0
+
779-76-0
反应条件
1,2,4,5-tetramethyl benzene; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane T=100°C; 11 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
694-80-4
2-溴氯苯
+
85199-06-0
→
反应条件
2523-39-9
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide T=140 - 150°C; 5 h;
参考文献
Liu, Tao-Ping; Xing, Chun-Hui; Hu, Qiao-Sheng
Angewandte Chemie - International Edition, 2010 , vol. 49, # 16 p. 2909 - 2912
1013-88-3
+
694-80-4
2-溴氯苯
→
反应条件
2720-93-6
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine in N,N-dimethyl acetamide T=170°C; 9 h; Inert atmosphere;
参考文献
Takeda, Daisuke; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Heterocycles, 2012 , vol. 86, # 1 p. 487 - 496
2398-37-0
+
694-80-4
2-溴氯苯
→
反应条件
24423-07-2
+
19493-33-5
2-氯-4'-甲基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 96 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
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