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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴氯苯
合成路线
（共 250 条）
108-86-1
溴代苯
→
反应条件
106-39-8
4-溴氯苯
+
106-46-7
对二氯苯
+
694-80-4
2-溴氯苯
+
106-37-6
对二溴苯
+
108-90-7
氯苯
+
583-53-9
1,2-二溴苯
反应条件
potassium chloride; cobalt(III) acetate; trifluoroacetic acid T=20°C; 15 h; Mn(CH3COO)3, 600 - 216 h, various conc. of aq. CF3COOH; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 609 - 615
Zhurnal Organicheskoi Khimii, , vol. 22, # 4 p. 681 - 688
7726-95-6
溴
+
108-90-7
氯苯
→
反应条件
694-80-4
2-溴氯苯
反应条件
暂无反应条件数据
参考文献
Journal of the Indian Chemical Society, , vol. 25, p. 277,280
Journal of the Indian Chemical Society, , vol. 26, p. 366
88400-64-0
+
108-88-3
甲苯
→
反应条件
106-39-8
4-溴氯苯
+
108-37-2
间氯溴苯
+
694-80-4
2-溴氯苯
+
100-39-0
溴化苄
+
103-29-7
1,2-二苯乙烷
+
108-90-7
氯苯
反应条件
T=55°C; 16 h; Irradiationother solvents; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 893 - 896
50-00-0
甲醛
+
54903-50-3
4,5,6,7-四氢噻吩并[3.2-c]吡啶
+
694-80-4
2-溴氯苯
→
反应条件
55142-85-3
噻氯匹定
反应条件
1: 1-bromo-2-chloro-benzene With ethylene dibromide; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile T=20°C; 0.5 h; Inert atmosphere; 2: formaldehyd; 4,5,6,7-tetrahydro-thieno[3,2-c]-pyridine in acetonitrile T=60°C; 1 h; Inert atmosphere;
参考文献
Isabelle, Aillaud; Haurena, Caroline; Gall, Erwan Le; Martens, Thierry; Ricci, Gino
Molecules, 2010 , vol. 15, # 11 p. 8144 - 8155
694-80-4
2-溴氯苯
+
461-96-1
1-溴-3,5-二氟苯
→
反应条件
372-18-9
1,3-二氟苯
+
108-90-7
氯苯
反应条件
1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=0°C; 2: With methanol in tetrahydrofuran Reactivity;
参考文献
Shi, Lei; Chu, Yuanyuan; Knoechel, Paul; Mayr, Herbert
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2760 - 2764
694-80-4
2-溴氯苯
+
64115-88-4
邻溴三氟甲氧基苯
→
反应条件
456-55-3
三氟甲氧基苯
+
108-90-7
氯苯
反应条件
1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=0°C; 2: With methanol in tetrahydrofuran Reactivity;
参考文献
Shi, Lei; Chu, Yuanyuan; Knoechel, Paul; Mayr, Herbert
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2760 - 2764
694-80-4
2-溴氯苯
+
21524-34-5
1-溴-2,4,6-三异丙苯
+
16523-54-9
二环己基氯化膦
→
反应条件
564483-18-7
2-二环己基磷-2,4,6-三异丙基联苯
反应条件
1: 2-bromo-1,3,5-triisopropylbenzene With magnesium; ethylene dibromide in tetrahydrofuran T=65°C; 1 h; 2: 1-bromo-2-chloro-benzene in tetrahydrofuran T=65°C; 1 h; 3: chloro-dicyclohexylphosphine With copper(l) chloride in tetrahydrofuran T=20°C; 20 h;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
694-80-4
2-溴氯苯
+
21524-34-5
1-溴-2,4,6-三异丙苯
+
100384-03-0
→
反应条件
564483-18-7
2-二环己基磷-2,4,6-三异丙基联苯
反应条件
1: 2-bromo-1,3,5-triisopropylbenzene With magnesium; ethylene dibromide in tetrahydrofuran T=65°C; Inert atmosphere; 2: 1-bromo-2-chloro-benzene in tetrahydrofuran T=65°C; 2 h; 3: dicyclohexylbromophosphine With copper(l) chloride in tetrahydrofuran T=20°C; 10 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
694-80-4
2-溴氯苯
→
反应条件
3900-89-8
2-氯苯基硼酸
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane; toluene T=-70°C; 1.5 h; Inert atmosphere;
参考文献
PHILADELPHIA HEALTH and EDUCATION CORPORATION; INSTITUTE FOR HEPATITIS AND VIRUS RESEARCH; KATSIKIS, Peter, D.; KINNEY, William, A.; ALMOND, Harold, R.; KHAN, Noshena
Patent: WO2013/90725 A1, 2013 ;
Location in patent: Page/Page column 68 ;
→
反应条件
3900-89-8
2-氯苯基硼酸
反应条件
magnesium in water
参考文献
Bristol-Myers Squibb Company
Patent: US6011029 A1, 2000 ;
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