(7CI,8CI,9CI)-2,3-二甲基喹噁啉 1-氧化物合成路线 (共 5 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 20 h;
参考文献
Liu, Gu; Botting, Catherine H.; Evans, Kathryn M.; Walton, Jeffrey A. G.; Xu, Guogang; Slawin, Alexandra M. Z.; Westwood, Nicholas J.
ChemMedChem, 2010 , vol. 5, # 1 p. 41 - 45
反应条件
ascorbic acid powder in water
T=90 - 95°C; 5 h;
参考文献
Novacek, Libor; Nechvatal, Miloslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 6 p. 1302 - 1306
反应条件
1: toluene / |Reflux
2: [bis(acetoxy)iodo]benzene / dichloromethane / 5 h / 20 °C
View Scheme
参考文献
Aggarwal, Ranjana; Rani, Chinu; Sumran, Garima
Synthetic Communications, 2014 , vol. 44, # 7 p. 923 - 928
参考文献
Kaupp, Gerd; Voss, Heike; Frey, Herbert
Angewandte Chemie, 1987 , vol. 99, # 12 p. 1327 - 1328
反应条件
T=190 - 195°C; 1 h; Product distribution;
参考文献
Hirota, Takashi; Namba, Tetsuto; Sasaki, Kenji
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 949 - 953