2-氨基-2,3-二氢-1H-茚-1-酮盐酸盐合成路线 （共 8 条）
反应条件
sodium ethanolate; sodium in ethanol; toluene
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4548943 A1, 1985 ;
反应条件
aluminium trichloride in carbon disulfide
T=50°C; 4 h;
参考文献
Effenberger, Franz; Steegmueller, Dieter; Null, Volker; Ziegler, Thomas
Chemische Berichte, 1988 , vol. 121, p. 125 - 130
反应条件
hydrogenchloride; acetic acid in water
T=110°C; 10 h;
参考文献
Zhao, Rong; Guo, Peijiang; Dong, Junyu; Zhang, Xiaoping; Sun, Xiaofei; Tian, Yun; Zeng, Qingle
Organic Preparations and Procedures International, 2011 , vol. 43, # 4 p. 377 - 380
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol; water
2 h;
参考文献
Hall, J. Herbert; Chien, Joseph Yuming; Kauffman, Joel M.; Litak, Peter T.; Adams, Jeffrey K.; et al.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1245 - 1273
反应条件
1: 1.) HCl, 2.) isoamyl nitrite / 1.) ether, 2.) ether,
2: 40 percent / 12 M HCl, H2 / 5percent Pd/C / H2O; methanol / 2 h
View Scheme
参考文献
Hall, J. Herbert; Chien, Joseph Yuming; Kauffman, Joel M.; Litak, Peter T.; Adams, Jeffrey K.; et al.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1245 - 1273
反应条件
1: PCl5 / CCl4 / 10 h
2: 49.8 percent / AlCl3 / CS2 / 4 h / 50 °C
View Scheme
参考文献
Petrovskaia; Taylor; Hauze; Carroll; Joullie
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7666 - 7675
反应条件
1: 61 percent / PCl5, CH3COCl
2: 75 percent / AlCl3 / CS2 / 4 h / 50 °C
View Scheme
参考文献
Effenberger, Franz; Steegmueller, Dieter; Null, Volker; Ziegler, Thomas
Chemische Berichte, 1988 , vol. 121, p. 125 - 130
反应条件
1: PPA / 3 h / 130 °C
2: hydrogenchloride; acetic acid / water / 10 h / 110 °C
View Scheme
参考文献
Zhao, Rong; Guo, Peijiang; Dong, Junyu; Zhang, Xiaoping; Sun, Xiaofei; Tian, Yun; Zeng, Qingle
Organic Preparations and Procedures International, 2011 , vol. 43, # 4 p. 377 - 380
